FTIR

Fourier Transform Infrared Spectroscopy
Last Updated: 20210317 mtim

Thermo Fisher IS50R Bench
Standard Operating Procedure (SOP)

Measurement Range: 12,500cm-1 to 50cm-1
Samples: Solids, Liquids and Gases
Measurement Modes: Transmission, Reflection ATR, Polarization, Emission & Time Dependent, Columated or Focused.

Bench Accessories:
Transmission
     Solids Typical Sample Size 1cm, 1mm minimum (with masking)
     Liquds
         Liquid Cell - Zinc Selenide Windows, Adjustable pathlength
         Demountable Liquid Cell
         Horizon - Horizontal Attenuated Total Reflecion Accessory
         Long Pathlength Glass Cell
         Cuvette Holder

     Gases
         Gas Cell

Specular Reflection
     ERA 12 deg
     ERA 80 deg
     ERA 85 deg
     VMax 30-80 deg
Diffuse Reflection
     Praying Mantis
Zinc Selenide Wire Grid Polarizer (25mm dia)

Attenuated Total Reflection (ATR)

     Diamond ATR - In the Bench (45 Degrees)
     Horizon - Horizontal Attenuated Total Reflecion Accessory
     Grazing Angle ATR, Germanium, 65 Degrees
     MIcro - ATR, Germanium, Sampling Area: 25x25um typical 
     4X Beam Condensor Transmission & ATR

Continuum FTIR Microscope
Measurement Range: 12,500 cm-1 to 400cm-1
Samples: Solids, Liquids and Gases.
Sampling Area: Adjustable 100um to 20um.
Measurement Modes: Transmission, Reflection ATR, Polarization, Mapping, Emission & Time Dependent.
Visible and Infrared Polarizers
Microscope Slide On ATR
Diamond Compression Cell
Contact Alert System
Temperature Controlled Microscope Stage
Refrachromat IR Objective: 15X/0.58 N.A
Zinc Selenide Wire Grid Polarizer (25mm dia).

Emission Port
     Bench
     Microscope

External Detector - Allows remote positioning of detector.

Detector Material Characterization Accessory - with and without amplifier

Sample Preperation Accesories:
Pellet Press
Ball Mill

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Thermo Fisher 6700 FTIR Bench - (Users should plan on getting trained on the new IS50 FTIR)
Standard Operating Procedure (SOP)

Measurement Range: 12,500cm-1 to 50cm-1
Samples: Solids, Liquids and Gases
Measurement Modes: Transmission, Reflection ATR, Polarization, Emission & Time Dependent.

Bench Accessories:
Transmission
     Solids Typical Sample Size 1cm, 1mm minimum (with masking)
     Liquds
         Liquid Cell - Zinc Selenide Windows, Adjustable pathlength
         Demountable Liquid Cell
         Horizon - Horizontal Attenuated Total Reflecion Accessory
         Long Pathlength Glass Cell
         Cuvette Holder

     Gases
         Gas Cell

Specular Reflection
     ERA 12 deg
     ERA 80 deg
     ERA 85 deg
     VMax 30-80 deg
Diffuse Reflection
     Praying Mantis

Attenuated Total Reflection (ATR)
     Horizon - Horizontal Attenuated Total Reflecion Accessory
     Grazing Angle ATR
     MIcro - ATR, Germanium Sampling Area: 25x25um typical
     4X Beam Condensor Transmission & ATR

Emission Port
     Bench
     Microscope

External Detector - Allows remote positioning of detector.

Detector Material Characterization Accessory - with and without amplifier

Sample Preperation Accessories:
Pellet Press
Ball Mill